异十三吗啉

  • 基本信息
  • 制备方法及用途
  • 物化性质
  • 安全信息
  • 毒理性
  • MSDS
  • 海关数据
  • 结构与计算化学
  • 表征图谱

异十三吗啉 基本信息

中文名称:
异十三吗啉 
中文别名:
异十三吗啉;
三缩吗吩醇;
克啉菌;
2,6-二甲基十三烷基吗啉;
克啉菌,三缩吗吩醇 
英文名称:
Morpholine,2,6-dimethyl-4-tridecyl-
英文别名:
Tridemorph;
N-Tridecyl-2,6-dimethylmorpholine;
Basf 220f;
CALIXIN;
e-236;
2,6-dimethyl-N-tridecylmorpholine;
TRIDEMORPN;
CALAXIN;
BAFS 220F;
bas2205-f;
Calixine;
2,6-dimethyl-4-tridecylmorpholine;
2,6-Dimethyl-4-tridecylmorpholine 
CAS No.:
24602-86-6
分 子 式:
C19H39NO
分 子 量:
297.52
精确分子量:
297.30300
PSA:
12.47000
MDL:
MFCD00055522
EINECS:
246-347-3
InChI:
The Key: YTOPFCCWCSOHFV-UHFFFAOYSA-N
危险品标志:
ToxicTDangerousNDangerousNToxicT
风险术语:
20/22-38-50/53-61
安全术语:
45-53-60-61
分子结构式:
SDS:
查看

异十三吗啉 制备方法及用途

制备方法

由N,N-双(β-羟丙基)十三胺在硫酸存在下,于160℃脱水环合制得。

合成制备方法

由N,N-双(β-羟丙基)十三胺在硫酸存在下,于160℃脱水环合制得。

用途简介

广谱内吸杀菌剂。主要用于防治麦类白粉病、叶锈病和条锈病。

用途

1.吗啉类杀菌剂,兼有保护、治疗和内吸作用,残效长,对作物无药害,用于防治大麦、小麦的白粉病,小麦叶锈病、条锈病,黄瓜、马铃薯、橡胶、豌豆的白粉病。

2.用作医药中间体

异十三吗啉 物化性质

密度:
0.856 g/cm3
沸点:
371.3ºC at 760 mmHg
闪点:
109.5ºC
折射率:
1.449
蒸汽压:
1.04E-05mmHg at 25°C
存储条件/存储方法:
库房通风低温干燥,与食品原料分开储运
稳定性相关:

纯品为无色油状液体,略有氨味。b.p.134℃/66.65Pa、 130~131℃/22.7Pa,蒸气压 1.27×10-2Pa (20℃)。能溶于丙酮、氯仿、苯、乙醇等有机溶剂,常温下在水中溶解度为0.01%。常温下贮存稳定

其它信息:

1.             性状:无色油状液体,略有氨味。

2.             密度(g/mL,20℃):不确定

3.             相对蒸汽密度(g/mL,空气=1):不确定

4.             熔点(ºC):134

5.             沸点(ºC):不确定

6.             折射率:不确定

7.             闪点(ºC):不确定

8.             比旋光度(ºC):不确定

9.             自燃点或引燃温度(ºC)不确定

10.          蒸气压(kPa,25ºC):1.27×10-2

11.          饱和蒸气压(kPa,60ºC):不确定

12.          燃烧热(KJ/mol):不确定

13.          临界温度(ºC):不确定

14.          临界压力(KPa):不确定

15.          油水(辛醇/水)分配系数的对数值:不确定

16.          爆炸上限(%,V/V):不确定

17.          爆炸下限(%,V/V):不确定

18.          溶解性:能溶于丙酮、氯仿、苯、乙醇等有机溶剂。

异十三吗啉 安全信息

包装等级:
III
风险类别:
6.1(b)
海关代码:
2934999035
危险类别码:
R20/22;R38;R50/53;R61
安全说明:
S45-S53-S60-S61
RTECS号:
QE2705000
安全标志:
S45:出现意外或者感到不适,立刻到医生那里寻求帮助(最好带去产品容器标签)。
S53:避免暴露——使用前先阅读专门的说明。
S60:本物质残余物和容器必须作为危险废物处理。
S61:避免排放到环境中。参考专门的说明/安全数据表。
危险标志:
T:Toxic; N:Dangerous for the environment;

异十三吗啉 毒理性

CHEMICAL IDENTIFICATION

RTECS NUMBER :
QE2705000
CHEMICAL NAME :
Morpholine, 2,6-dimethyl-N-tridecyl-
CAS REGISTRY NUMBER :
24602-86-6
LAST UPDATED :
199706
DATA ITEMS CITED :
11
MOLECULAR FORMULA :
C19-H39-N-O
MOLECULAR WEIGHT :
297.59
WISWESSER LINE NOTATION :
T6N DOTJ A13 C1 F1

HEALTH HAZARD DATA

ACUTE TOXICITY DATA

TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE :
Oral
SPECIES OBSERVED :
Rodent - rat
DOSE/DURATION :
650 mg/kg
TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value
REFERENCE :
GUCHAZ Guide to the Chemicals Used in Crop Protection. (Information Canada, 171 Slater St., Ottawa, Ont., Canada) Volume(issue)/page/year: 6,522,1973
TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE :
Oral
SPECIES OBSERVED :
Rodent - mouse
DOSE/DURATION :
1560 mg/kg
TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value
REFERENCE :
VPITAR Voprosy Pitaniya. Problems of Nutrition. (V/O Mezhdunarodnaya Kniga, 113095 Moscow, USSR) V.1-10, 1932-41; V.11- 1952- Volume(issue)/page/year: 39(6),55,1981
TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE :
Oral
SPECIES OBSERVED :
Mammal - cat
DOSE/DURATION :
540 mg/kg
TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value
REFERENCE :
VPITAR Voprosy Pitaniya. Problems of Nutrition. (V/O Mezhdunarodnaya Kniga, 113095 Moscow, USSR) V.1-10, 1932-41; V.11- 1952- Volume(issue)/page/year: 39(6),55,1981
TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE :
Oral
SPECIES OBSERVED :
Rodent - rabbit
DOSE/DURATION :
750 mg/kg
TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value
REFERENCE :
28ZEAL "Pesticide Index," Frear, E.H., ed., State College, PA, College Science Pub., 1969 Volume(issue)/page/year: 5,229,1976
TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE :
Oral
SPECIES OBSERVED :
Rodent - guinea pig
DOSE/DURATION :
1 gm/kg
TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value
REFERENCE :
VPITAR Voprosy Pitaniya. Problems of Nutrition. (V/O Mezhdunarodnaya Kniga, 113095 Moscow, USSR) V.1-10, 1932-41; V.11- 1952- Volume(issue)/page/year: 39(6),55,1981 ** REPRODUCTIVE DATA **
TYPE OF TEST :
TDLo - Lowest published toxic dose
ROUTE OF EXPOSURE :
Oral
DOSE :
1300 mg/kg
SEX/DURATION :
female 1-20 day(s) after conception
TOXIC EFFECTS :
Reproductive - Specific Developmental Abnormalities - homeostasis
REFERENCE :
VPITAR Voprosy Pitaniya. Problems of Nutrition. (V/O Mezhdunarodnaya Kniga, 113095 Moscow, USSR) V.1-10, 1932-41; V.11- 1952- Volume(issue)/page/year: 39(6),55,1981
TYPE OF TEST :
TDLo - Lowest published toxic dose
ROUTE OF EXPOSURE :
Oral
DOSE :
5400 ug/kg
SEX/DURATION :
female 7-15 day(s) after conception
TOXIC EFFECTS :
Reproductive - Specific Developmental Abnormalities - other developmental abnormalities
REFERENCE :
VPITAR Voprosy Pitaniya. Problems of Nutrition. (V/O Mezhdunarodnaya Kniga, 113095 Moscow, USSR) V.1-10, 1932-41; V.11- 1952- Volume(issue)/page/year: 38(6),51,1980
TYPE OF TEST :
TDLo - Lowest published toxic dose
ROUTE OF EXPOSURE :
Oral
DOSE :
29250 ug/kg
SEX/DURATION :
female 7-15 day(s) after conception
TOXIC EFFECTS :
Reproductive - Specific Developmental Abnormalities - Central Nervous System Reproductive - Specific Developmental Abnormalities - urogenital system
REFERENCE :
VPITAR Voprosy Pitaniya. Problems of Nutrition. (V/O Mezhdunarodnaya Kniga, 113095 Moscow, USSR) V.1-10, 1932-41; V.11- 1952- Volume(issue)/page/year: 39(6),55,1981
TYPE OF TEST :
TDLo - Lowest published toxic dose
ROUTE OF EXPOSURE :
Oral
DOSE :
585 mg/kg
SEX/DURATION :
female 7-15 day(s) after conception
TOXIC EFFECTS :
Reproductive - Specific Developmental Abnormalities - craniofacial (including nose and tongue)
REFERENCE :
VPITAR Voprosy Pitaniya. Problems of Nutrition. (V/O Mezhdunarodnaya Kniga, 113095 Moscow, USSR) V.1-10, 1932-41; V.11- 1952- Volume(issue)/page/year: 39(6),55,1981
TYPE OF TEST :
TDLo - Lowest published toxic dose
ROUTE OF EXPOSURE :
Oral
DOSE :
5400 ug/kg
SEX/DURATION :
female 7-15 day(s) after conception
TOXIC EFFECTS :
Reproductive - Specific Developmental Abnormalities - cardiovascular (circulatory) system
REFERENCE :
VPITAR Voprosy Pitaniya. Problems of Nutrition. (V/O Mezhdunarodnaya Kniga, 113095 Moscow, USSR) V.1-10, 1932-41; V.11- 1952- Volume(issue)/page/year: 39(6),55,1981
TYPE OF TEST :
TDLo - Lowest published toxic dose
ROUTE OF EXPOSURE :
Oral
DOSE :
2451 mg/kg
SEX/DURATION :
female 6-15 day(s) after conception
TOXIC EFFECTS :
Reproductive - Specific Developmental Abnormalities - craniofacial (including nose and tongue)
REFERENCE :
TJADAB Teratology, The International Journal of Abnormal Development. (Alan R. Liss, Inc., 41 E. 11th St., New York, NY 10003) V.1- 1968- Volume(issue)/page/year: 29,259,1984
毒理学数据:

大鼠急性经口LD50>1000mg/kg(558mg/kg,原油),兔急性经口LD50750mg/kg。大鼠急性经皮LD50>4000mg/kg,急性吸入LC504.5mg/L。大鼠亚慢性无作用剂量为50mg/kg,狗为800mg/kg。大鼠慢性无作用剂量为80mg/kg,小鼠为90mg/kg。将大鼠置于十三吗啉饱和的空气,8h后未见死亡。大剂量(220L/kg)有致畸和繁殖毒性,低剂量(24L/kg)无影响。没有致突变和致癌作用。
加入二氯二异丙醚360kg,合成C11~C13脂肪胺120kg,液碱140kg,水100kg,搅拌下于95℃反应4h,继续升温至110℃反应1h,反应结束。静置分层,水相送往三废处理,油相进行蒸馏,负压稳定在2.67kPa,回流比1:1~2:1,截取塔顶温度为83~86℃馏分回收醚,100~160℃馏分回收胺,160~200℃馏分得十三吗啉。以胺计收率≥80%,含量≥95%。

异十三吗啉 MSDS


Section 1. IDENTIFICATION OF THE SUBSTANCE/MIXTURE
  Product identifiers
    Product name        : Tridemorph    
    CAS-No.        : 24602-86-6    
  Relevant identified uses of the substance or mixture and uses advised against
    Identified uses        : Laboratory chemicals, Manufacture of substances    
  
  

Section 2. HAZARDS IDENTIFICATION
  Classification of the substance or mixture
  Classification according to Regulation (EC) No 1272/2008 [EU-GHS/CLP]
    Reproductive toxicity (Category 1B)
    Acute toxicity, Inhalation (Category 4)
    Acute toxicity, Oral (Category 4)
    Skin irritation (Category 2)
    Acute aquatic toxicity (Category 1)
    Chronic aquatic toxicity (Category 1)
  Classification according to EU Directives 67/548/EEC or 1999/45/EC
    May cause harm to the unborn child. Harmful by inhalation and if swallowed. Irritating to skin. Very toxic to
    aquatic organisms, may cause long-term adverse effects in the aquatic environment.
  Label elements
  Labelling according Regulation (EC) No 1272/2008 [CLP]
    Pictogram
    Signal word        Danger    
    Hazard statement(s)
    H315        Causes skin irritation.    
    H302        Harmful if swallowed.    
    H332        Harmful if inhaled.    
    H410        Very toxic to aquatic life with long lasting effects.    
    H360D        May damage the unborn child.    
    Precautionary statement(s)
    P201        Obtain special instructions before use.    
    P273        Avoid release to the environment.    
    P308 + P313        IF exposed or concerned: Get medical advice/ attention.    
    P501        Dispose of contents/ container to an approved waste disposal plant.    
    Supplemental Hazard        none    
    Statements
  According to European Directive 67/548/EEC as amended.
    Hazard symbol(s)
    R-phrase(s)
    R61        May cause harm to the unborn child.    
    R20/22        Also harmful by inhalation and if swallowed.    
    R38        Irritating to skin.    
    R50/53        Very toxic to aquatic organisms, may cause long-term adverse effects in    
    the aquatic environment.
    S-phrase(s)
    S53        Avoid exposure - obtain special instructions before use.    
    S45        In case of accident or if you feel unwell, seek medical advice immediately    
    (show the label where possible).
    S60        This material and its container must be disposed of as hazardous waste.    
    S61        Avoid release to the environment. Refer to special instructions/ Safety    
    data sheets.
    Restricted to professional users.
  Other hazards - none

Section 3. COMPOSITION/INFORMATION ON INGREDIENTS
  Substances
    Formula        : C19H39NO    
    Molecular Weight        : 297,52 g/mol    
    Component        Concentration    
  Tridemorph
    CAS-No.        24602-86-6        -    
    EC-No.        246-347-3    
    Index-No.        613-020-00-5    

Section 4. FIRST AID MEASURES
  Description of first aid measures
  General advice
    Consult a physician. Show this safety data sheet to the doctor in attendance.
  If inhaled
    If breathed in, move person into fresh air. If not breathing, give artificial respiration. Consult a physician.
  In case of skin contact
    Wash off with soap and plenty of water. Consult a physician.
  In case of eye contact
    Flush eyes with water as a precaution.
  If swallowed
    Never give anything by mouth to an unconscious person. Rinse mouth with water. Consult a physician.
  Most important symptoms and effects, both acute and delayed
  Indication of any immediate medical attention and special treatment needed
    no data available

Section 5. FIREFIGHTING MEASURES
  Extinguishing media
  Suitable extinguishing media
    Use water spray, alcohol-resistant foam, dry chemical or carbon dioxide.
  Special hazards arising from the substance or mixture
    Carbon oxides, nitrogen oxides (NOx)
    Carbon oxides, nitrogen oxides (NOx)
  Advice for firefighters
    Wear self contained breathing apparatus for fire fighting if necessary.
  Further information
    no data available

Section 6. ACCIDENTAL RELEASE MEASURES
  Personal precautions, protective equipment and emergency procedures
    Use personal protective equipment. Avoid breathing vapors, mist or gas. Ensure adequate ventilation.
    Evacuate personnel to safe areas.
  Environmental precautions
    Prevent further leakage or spillage if safe to do so. Do not let product enter drains. Discharge into the
    environment must be avoided.
  Methods and materials for containment and cleaning up
    Soak up with inert absorbent material and dispose of as hazardous waste. Keep in suitable, closed
    containers for disposal.
  Reference to other sections
    For disposal see section 13.

Section 7. HANDLING AND STORAGE
  Precautions for safe handling
    Avoid exposure - obtain special instructions before use.Avoid contact with skin and eyes. Avoid inhalation
    of vapour or mist.
  Conditions for safe storage, including any incompatibilities
    Store in cool place. Keep container tightly closed in a dry and well-ventilated place. Containers which are
    opened must be carefully resealed and kept upright to prevent leakage.
  Specific end uses
    no data available

Section 8. EXPOSURE CONTROLS/PERSONAL PROTECTION
  Control parameters
  Components with workplace control parameters
  Exposure controls
  Appropriate engineering controls
    Handle in accordance with good industrial hygiene and safety practice. Wash hands before breaks and
    at the end of workday.
  Personal protective equipment
  Eye/face protection
    Face shield and safety glasses Use equipment for eye protection tested and approved under
    appropriate government standards such as NIOSH (US) or EN 166(EU).
  Skin protection
    Handle with gloves. Gloves must be inspected prior to use. Use proper glove removal technique
    (without touching glove's outer surface) to avoid skin contact with this product. Dispose of
    contaminated gloves after use in accordance with applicable laws and good laboratory practices.
    Wash and dry hands.
    The selected protective gloves have to satisfy the specifications of EU Directive 89/686/EEC and
    the standard EN 374 derived from it.
  Body Protection
    Complete suit protecting against chemicals, The type of protective equipment must be selected
    according to the concentration and amount of the dangerous substance at the specific workplace.
  Respiratory protection
    Where risk assessment shows air-purifying respirators are appropriate use a full-face respirator
    with multi-purpose combination (US) or type ABEK (EN 14387) respirator cartridges as a backup
    to engineering controls. If the respirator is the sole means of protection, use a full-face supplied air
    respirator. Use respirators and components tested and approved under appropriate government
    standards such as NIOSH (US) or CEN (EU).

Section 9. PHYSICAL AND CHEMICAL PROPERTIES
  Information on basic physical and chemical properties
    a) Appearance        Form: liquid    
    Colour: colourless
    b) Odour        no data available    
    c) Odour Threshold        no data available    
    d) pH        no data available    
    e) Melting point/freezing        no data available    
    point
    f) Initial boiling point and 134 °C at 0,7 hPa
    boiling range
    g) Flash point        no data available    
    h) Evaporation rate        no data available    
    i) Flammability (solid, gas) no data available
    j) Upper/lower        no data available    
    flammability or
    explosive limits
    k) Vapour pressure        no data available    
    l) Vapour density        no data available    
    m) Relative density        no data available    
    n) Water solubility        insoluble    
    o) Partition coefficient: n- no data available
    octanol/water
    p) Autoignition        no data available    
    temperature
    q) Decomposition        no data available    
    temperature
    r) Viscosity        no data available    
    s) Explosive properties        no data available    
    t) Oxidizing properties        no data available    
  Other safety information
    no data available

Section 10. STABILITY AND REACTIVITY
  Reactivity
    no data available
  Chemical stability
    no data available
  Possibility of hazardous reactions
    no data available
  Conditions to avoid
    no data available
  Incompatible materials
    Strong oxidizing agents
  Hazardous decomposition products
    Other decomposition products - no data available

Section 11. TOXICOLOGICAL INFORMATION
  Information on toxicological effects
  Acute toxicity
    LD50 Oral - rat - 650 mg/kg
  Skin corrosion/irritation
    no data available
  Serious eye damage/eye irritation
    no data available
  Respiratory or skin sensitization
    no data available
  Germ cell mutagenicity
    no data available
  Carcinogenicity
    IARC:        No component of this product present at levels greater than or equal to 0.1% is identified as    
    probable, possible or confirmed human carcinogen by IARC.
  Reproductive toxicity
    Presumed human reproductive toxicant
    Developmental Toxicity - rat - Oral
    Specific Developmental Abnormalities: Central nervous system. Specific Developmental Abnormalities:
    Urogenital system.
    Developmental Toxicity - rat - Oral
    Specific Developmental Abnormalities: Craniofacial (including nose and tongue).
    Developmental Toxicity - rat - Oral
    Specific Developmental Abnormalities: Cardiovascular (circulatory) system.
    Developmental Toxicity - rat - Oral
    Specific Developmental Abnormalities: Homeostasis
    Developmental Toxicity - mouse - Oral
    Specific Developmental Abnormalities: Craniofacial (including nose and tongue).
  Specific target organ toxicity - single exposure
    no data available
  Specific target organ toxicity - repeated exposure
    no data available
  Aspiration hazard
    no data available
  Potential health effects
  Inhalation        Harmful if inhaled. Causes respiratory tract irritation.    
  Ingestion
    Harmful if swallowed.
  Skin        May be harmful if absorbed through skin. Causes skin irritation.    
  Additional Information
    RTECS: QE2705000

Section 12. ECOLOGICAL INFORMATION
  Toxicity
    no data available
  Persistence and degradability
    no data available
  Bioaccumulative potential
    no data available
  Mobility in soil
    no data available
  Results of PBT and vPvB assessment
    no data available
  Other adverse effects
    Very toxic to aquatic life.

Section 13. DISPOSAL CONSIDERATIONS
  Waste treatment methods
  Product
    Offer surplus and non-recyclable solutions to a licensed disposal company.
  Contaminated packaging
    Dispose of as unused product.

Section 14. TRANSPORT INFORMATION
  UN number
    ADR/RID: 3082        IMDG: 3082        IATA: 3082    
  UN proper shipping name
    ADR/RID: ENVIRONMENTALLY HAZARDOUS SUBSTANCE, LIQUID, N.O.S. (Tridemorph)
    IMDG: ENVIRONMENTALLY HAZARDOUS SUBSTANCE, LIQUID, N.O.S. (Tridemorph)
    IATA:        Environmentally hazardous substance, liquid, n.o.s. (Tridemorph)    
  Transport hazard class(es)
    ADR/RID: 9        IMDG: 9        IATA: 9    
  Packaging group
    ADR/RID: III        IMDG: III        IATA: III    
  Environmental hazards
    ADR/RID: yes        IMDG Marine pollutant: yes        IATA: yes    
  Special precautions for user
  Further information
    EHS-Mark required (ADR 2.2.9.1.10, IMDG code 2.10.3) for single packagings and combination
    packagings containing inner packagings with Dangerous Goods > 5L for liquids or > 5kg for solids.

Section 15. REGULATORY INFORMATION
    This safety datasheet complies with the requirements of Regulation (EC) No. 1907/2006.
  Safety, health and environmental regulations/legislation specific for the substance or mixture
    no data available
  Chemical Safety Assessment
    no data available

Section 16. OTHER INFORMATION
  Further information
    Copyright 2012 Co. LLC. License granted to make unlimited paper copies for internal use
    only.
    The above information is believed to be correct but does not purport to be all inclusive and shall be
    used only as a guide. The information in this document is based on the present state of our knowledge
    and is applicable to the product with regard to appropriate safety precautions. It does not represent any
    guarantee of the properties of the product. Corporation and its Affiliates shall not be held
    liable for any damage resulting from handling or from contact with the above product. See
     and/or the reverse side of invoice or packing slip for additional terms and conditions of sale.

异十三吗啉 海关数据

中国海关编码:2934999035

概述:
2934999035 十二环吗啉,十三吗啉。监管条件:S(进出口农药登记证明)。增值税率:17.0%。退税率:9.0%。最低关税:6.5%。普通关税:20.0%
申报要素:
品名, 成分含量, 用途
监管条件:
S.进出口农药登记证明
摘要/Summary:
2934999035 2,6-dimethyl-4-tridecylmorpholine。supervision conditions:s(import or export registration certificate for pesticides)。VAT:17.0%。tax rebate rate:9.0%。MFN tarrif:6.5%。general tariff:20.0%

异十三吗啉 分子结构与计算化学数据

分子结构数据

1、                           摩尔折射率:93.32

2、                           摩尔体积(cm3/mol):347.6

3、                           等张比容(90.2K):804.2

4、                           表面张力(dyne/cm):28.6

5、                          极化率(10-24cm3):36.99

异十三吗啉 表征图谱

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